AMS SYSTEMS

Principles of Operation

Accelerator Mass Spectrometry is the counting of individual nuclei. The sample is put into a negative ion source. The negative ions are injected into the positive terminal of an accelerator where all molecular ions are broken up and positive ions are formed. The positive ions are again accelerated and mass/energy analyzed to separate the abundant and rare isotopes.

See step #1 See step #2 See step #3 See step #4 See step #5 See step #6 See step #7
Pelletron AMS System

1. The negative ion source holds up to 40 or 133 samples. The samples can be either solid or gas. For carbon, the source produces a beam of carbon isotopes (12C, 13C, 14C) and negatively charged molecules. This source is also suitable for studies with other radioisotopes.

Negative ion source principles of operation




The ionizer produces a cesium beam which strikes the cooled sample surface. As particles from the sample are sputtered through the cesium, negative ions are formed.





2. The 90o magnet injection system sends individual isotopes into the accelerator sequentially by biasing the insulated magnet chamber. The voltage on the chamber is changed many times per second. Simultaneous injector systems are also available which separate the isotopes for mass selection and recombines them prior to acceleration.

3. The tandem Pelletron accelerates the negative ions to the positive terminal. In the terminal, stripper gas interacts with the negative ion beam to break up all molecules and produce positive ions. The positive ions then exit the positive terminal and are accelerated a second time to very high energies.

The stripper in the high voltage terminal




In the high voltage terminal, negatively charged ions and molecules enter the gas stripper assembly and positively charged ions exit. The stripper gas is recirculated in order to maintain the best possible vacuum conditions in the acceleration tube.




4. The positive ions are accelerated into the 90o mass/energy analysis magnet which separates the isotope beams for measurement.

Separation in the bending magnet





The ions entering the magnet are separated according to mE/q2: the ion mass multiplied by its energy divided by the square of its charge.







5. The offset Faraday cup assembly measures the abundant isotopes, 12C and 13C, which are deflected more than the heavier rare isotope 14C. The same principle holds for beryllium, aluminum, iodine, chlorine and other beam species.

6. The rare isotopes are transported through a 20o electrostatic deflector to filter out any other possible interfering ions for an overall system sensitivity of better than 1 out of 1015. Interfering background levels are reduced to a few parts in 1016.

7. The deflector counts the rare isotope and a computer calculates the fraction of rare isotope in each sample. In this way, ratios of 12C/14C and 13C/14C are measured. Precisions of better than 0.3% are routinely obtained.

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National Electrostatics Corporation
Last revised December 4, 2001 by Tim Davis, nec@pelletron.com
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URL: http://www.pelletron.com/amsop.htm